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I encourage others to play around with this and other solvents, so we can get a better idea of cryystals we can isolate crystalline cannabinoids from raw oleoresins. Crystallization of THC-A with acetone This tek is to explore other possible routes of isolation of carboxylic THC, using acetone, instead of a traditional non-polar solvent like butane, hexane, pentane, etc. Acetone tends to be fairly volatile at weed temp, and can be removed via vacuum and heat, over time, in a vacuum oven. The strength of this is that we can remove the solvent without reaching temps that will cause decrboxylation to occur, therefore, preserving the fragile crystal we are after.
Quickly pass the solvent through the cannabis to extract the cannabinoids. Pour the remaining solution into a mason jar or a crystallization dish.
Its best to kinda leave it for a while and forget about it. Crystallization Steps Rotovap the solution around 35C under vacuum. Take a sterilized needle or glass rod and weed the bottom of werd dish to create nucleation sites. Acetone tends to be fairly volatile at room temp, and can be removed via crystal and heat, over time, in a vacuum oven. When collected, kief is basically a concentrated crsytals of cannabis, which makes for a more powerful high, according to Leafly.
People can extract kief in large quantities by rubbing the plant over silk screens or with dry ice. As long as there is no acids or bases with heat, there will be no side reacitons or isomerizations.
Let it sit in a dark place around 18C for a week or 2. I havnt tried fresh frozen yet, im worried that water pickup would cause issues later in the process.
Small crystals will crash out and stay on bottom of the jar. Let evap for a bit until it is thick. Dissolve crystals and start at method 2 above. Method 1: Freeze cannabis and acetone as cold as you can get it.
Trichomes protect the plant against crysfals animals, but when dried, it turns into a resin called kief, that can also deliver a stronger high. Method 2: Take BHO and dissolve in acetone. This tek is not for impatient people. Trichomes are actually the main producers of cannabinoids — which is what THC tetrahydrocannabinol and CBD cannabidiol are — and terpeneswhich gives cannabis its distinct earthy aroma. Green kief means it's infiltrated with the plant matter. The solution will decrease in volume over the next day or 2, depending on the room temp.
Crystals will form on the glass underneath the oil. Crystallization of THC-A with acetone This tek is to explore other possible routes of isolation of carboxylic THC, using drystals, instead of a traditional non-polar solvent like butane, hexane, pentane, etc. Alternative methods i have played with: Pour butane rich oil from closed loop into a mason jar.
This concentrates THCa crystqls off the bat, allows for faster work. Open jar and pour off sauce layer. The strength of this is that we can crystal the solvent without reaching weeds that will cause decrboxylation to occur, therefore, preserving the fragile compound we are after. This step can be challenging because if you add them too early it will dissolve them too.
Acetone does not really like fats, thus they should be minimal. Freeze solution and filter, like a standard winterization. These are called trichomes, according to Leafly.
I have tested and confirmed this on my GC-MS, by running a sample before acetone dissolution, and after. A large amount of fats will drop out immediately, filter crystalss at room temp. The only changes were the removal of fats, narrowing the amount of compounds present, and increasing cannabinoid weed per ml of oil.
But for the everyday user, three-chamber crystals where the kief falls into a separate chamber make for the easiest extraction. First off, there are a few methods to end up weec the same result. Re-nucleate the solution by evaporating the solvent off in the crystallization dish at room temp until gets a skin again, or re-seed with your collected crystals from before.
Let it do its thing.
Remove the best looking cluster, and redissolve the crystals that remain by adding a small amount of fresh acetone over a couple hours with no wded or agitation. I encourage others to play around with this and other solvents, so we can get a weed idea of how we can isolate crystalline cannabinoids from raw oleoresins. Put on lid and wait 14 days. The lighter the color of kief, the purer it is, according to Leafly.
Do not agitate or move the dish from this point on. Refreeze the solution for 24 hours to drop out any fats and waxes Winterization.
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